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Analytical Method & Instrumentation Standard:ICP-MS per ICH Q3D(R2) / USP Instrument:Agilent 7900 ICP-MS (SN: JP32905) with He collision mode Sample Preparation:Closed-vessel microwave digestion (CEM MARS 6): 19.2 mg + 5 mL HNO (suprapure) + 1 mL HO (30%) Digestion Program:Ramp 20 min 200C, hold 15 min, cool to RT, dilute to 50.0 mL (Milli-Q) Calibration:Multi-element std (NIST SRM 3100 series), 5-point external cal